Characterization of shale formation of abandoned petroleum wells and treatment using acid simulation technique

Authors

DOI:

https://doi.org/10.15587/2706-5448.2021.227619

Keywords:

shale technology, carbonate reservoirs, Energy Dispersive X-ray, X-ray diffraction, Fourior Transformation Infra-Red

Abstract

The object of research is shale, which is a combination of carbonate (calcite or dolomite), and non clay minerals such as silica (quartz) and clay minerals such as kaolinite. Characterization of various minerals in shale formed in six abandoned petroleum wells was done using Energy Dispersive X-ray (EDX), X-ray diffraction (XRD) and Fourier Transformation Infra-Red (FTIR). Shale may contain a wide variety of minerals. The shale formation within the abandoned wells in the current study is at a deep of about (2600±300) meters. Three shale formation samples were collected from each of the abandoned wells. Characterizing the constituents of the clay minerals of the shale is important in the drilling and the treatment process.

The analyses declared that, some shale formation samples are similar. The study was continued on three abandoned petroleum wells (I, II and III). The XRD and FTIR obtained results of shale analysis show the existence of calcite (CaCO3) and quartz (SiO2) in the shale samples. Dolomite CaMg(CO3)2 is present in well (II) and well (III), and muscovite H2KAl3Si3O12 is present in well (I). Also, Kaolinite Al2Si2O5(OH)4, and barite (BaSO4) components are detected in the FTIR results. Mg, K, Al and Ba trace elements are detected by EDX analyses and may contribute chemically.

Shale technology and research development is concern with three steps: Characterization, simulation, and permeability stimulation. The present study focusing on the characterization and simulation of the shale formed in six abandoned (non-producing) petroleum wells for enhancing the productivity of carbonate reservoirs.

Author Biographies

Saleh Mahmoud Abdou, National Centre for Radiation Research and Technology, Atomic Energy Authority (AEA)

Radiation Physics Department

Nabila Amin Ali, Suez Oil Processing Company (SOPC)

Petroleum Engineering Department

Mohamed Rajaa Balboul, National Centre for Radiation Research and Technology, Atomic Energy Authority (AEA)

Solid State Physics Department

References

  1. Jordá, J. D., Jordán, M. M., Ibanco-Cañete, R., Montero, M. A., Reyes-Labarta, J. A., Sánchez, A., Cerdán, M. (2015). Mineralogical analysis of ceramic tiles by FTIR: A quantitative attempt. Applied Clay Science, 115, 1–8. doi: http://doi.org/10.1016/j.clay.2015.07.005
  2. Bhargava, S., Awaja, F., Subasinghe, N. (2005). Characterisation of some Australian oil shale using thermal, X-ray and IR techniques. Fuel, 84 (6), 707–715. doi: http://doi.org/10.1016/j.fuel.2004.11.013
  3. Wang, D.-M., Xu, Y.-M., He, D.-M., Guan, J., Zhang, O.-M. (2009). Investigation of mineral composition of oil shale. Asia-Pacific Journal of Chemical Engineering, 4 (5), 691–697. doi: http://doi.org/10.1002/apj.319
  4. Tissot, B. P., Welte, D. H. (1978). Petroleum Formation and Occurrence. Berlin, Heidelberg, New York: Springer Verlag. doi: http://doi.org/10.1007/978-3-642-96446-6
  5. Ji, J., Ge, Y., Balsam, W., Damuth, J. E., Chen, J. (2009). Rapid identification of dolomite using a Fourier Transform Infrared Spectrophotometer (FTIR): A fast method for identifying Heinrich events in IODP Site U1308. Marine Geology, 258 (1-4), 60–68. doi: http://doi.org/10.1016/j.margeo.2008.11.007
  6. Deaton, B. C., Balsam, W. L. (1991). Visible spectroscopy; a rapid method for determining hematite and goethite concentration in geological materials. Journal of Sedimentary Research, 61 (4), 628–632. doi: http://doi.org/10.1306/d4267794-2b26-11d7-8648000102c1865d
  7. Ruessink, B. H., Harville, D. G. (1992). Quantitative Analysis of Bulk Mineralogy: The Applicability and Performance of XRD and FTIR. Paper SPE 23828. SPE International Symposium on Formation Damage Control. Lafayette, 533–546. doi: http://doi.org/10.2118/23828-ms
  8. Kumar, R., Bansal, V., Badhe, R. M., Madhira, I. S. S., Sugumaran, V., Ahmed, S. et. al. (2013). Characterization of Indian origin oil shale using advanced analytical techniques. Fuel, 113, 610–616. doi: http://doi.org/10.1016/j.fuel.2013.05.055
  9. Vaculikova, L., Plevova, E. (2005). Identification of clay minerals and micas in sedimentary rocks. Acta Geodynamica et Geomaterialia, 2 (2 (138)), 167–175.
  10. Davies, S., Kelkar, S. (2007). Carbonate Stimulation. Middle East and Asia Reservoir Review, 8. Available at: https://www.academia.edu/36119228/CARBONATE_STIMULATION
  11. Kamal, M. S., Mahmoud, M., Hanfi, M., Elkatatny, S., Hussein, I. (2018). Clay minerals damage quantification in sandstone rocks using core flooding and NMR. Journal of Petroleum Exploration and Production Technology, 9 (1), 593–603. doi: http://doi.org/10.1007/s13202-018-0507-7
  12. Aqui, A. R., Zarrouk, S. (2011). Permeability enhancement of conventional geothermal well. New Zealand Geothermal Workshop 2011 Proceedings. Auckland. Available at: https://www.researchgate.net/publication/269395872
  13. Economides, M. J., Nolte, K. G. (2000). Reservoir stimulation. Wiley. Available at: https://www.researchgate.net/file.PostFileLoader.html?id=591b038148954c7bac0eeb2d&assetKey=AS%3A494639238529025%401494942593011
  14. Palharini Schwalbert, M., Aljawad, M. S., Hill, A. D., Zhu, D. (2020). Decision Criterion for Acid-Stimulation Method in Carbonate Reservoirs: Matrix Acidizing or Acid Fracturing? SPE Journal, 25 (5), 2296–2318. doi: http://doi.org/10.2118/199236-pa
  15. Test method LS-613 (1996). Method of test for determination of insoluble residue of carbonate aggregates. Rev. No. 16, 1–6.
  16. ASTM Designation D 3042 (Mn/DOT Modified), Lab manual (2000). Determination of acid insoluble residue in limestone and dolostone. Available at: https://www.dot.state.mn.us/materials/manuals/laboratory/1221.pdf
  17. Database of ATR-FT-IR spectra of various materials of conservation related materials in the MID-IR region. Available at: https://spectra.cs.ut.ee/
  18. Linga Raju, C., Narasimhulu, K., Gopal, N., Rao, J., Reddy, B. C. (2002). Electron paramagnetic resonance, optical and infrared spectral studies on the marine mussel Arca burnesi shells. Journal of Molecular Structure, 608 (2-3), 201–211. doi: http://doi.org/10.1016/s0022-2860(01)00952-8
  19. Farmer, V. C. (1974). The Infrared Spectra of Minerals. Mineralogical Society. London. Available at: https://agris.fao.org/agris-search/search.do?recordID=US201300534379
  20. Prost, R., Dameme, A., Huard, E., Driard, J., Leydecker, J. P. (1989). Infrared study of structural OH in kaolinite, dickite, nacrite, and poorly crystalline kaolinite at 5 to 600 K. Clays & Clay Minerals, 37, 464–468. doi: http://doi.org/10.1346/ccmn.1989.0370511

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Published

2021-04-30

How to Cite

Abdou, S. M., Ali, N. A., & Balboul, M. R. (2021). Characterization of shale formation of abandoned petroleum wells and treatment using acid simulation technique. Technology Audit and Production Reserves, 2(3(58), 20–24. https://doi.org/10.15587/2706-5448.2021.227619

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Section

Chemical and Technological Systems: Reports on Research Projects