Failure analysis of geothermal perforated casing tubing in H2S and O2 containing environment

Authors

DOI:

https://doi.org/10.15587/1729-4061.2020.215163

Keywords:

corrosion, H2S, air drilling, failure, tubing, failure analysis, carbon steel

Abstract

A failure incident occurred on perforated casing tubing for geothermal wells. The damage happened during the drilling process by an air drilling technique after eleven days from the installation. Even though air drilling is a common method for geothermal drilling, this incident showed a lesson to learn to prevent a similar accident in the future. Failure analysis based on the laboratory and field observation was done to get the failure incident's root cause. The visual identification result showed a severe depletion and cracks in the tubing at a depth of 1,450–1,500 m. Optical emission spectroscopy and the tensile test showed materials appropriateness to the specifications. The corrosion attacked from the outer side of the tube. This tubing was exposed to an environment with significant H2S, CO2, water steam, and oxygen from the air drilling process. The results of X-ray diffraction analysis (XRD) showed FeS and Fe3O4 in the corrosion product. Both of the scale formed as a different layer, where the FeS is formed below the Fe3O4 layer. The energy dispersive spectroscopy (EDS) results revealed that each tubing's sulfur content gets an increase in the deeper location. The gas sampling result showed that H2S gas is more dominant than CO2 gas, which showed the sour service condition. Corrosion rate calculation modeling was also performed based on the environment parameter; the result is lower than the real cases. The oxygen from air drilling also accelerates the corrosion rate as it acted as an oxidizing agent in the process. Free sulfur is possibly formed, which is possibly transformed into sulfuric acid. This study showed the lesson learn about the deadly combination of sulfur, oxygen, H2S, and CO2, making a severe corrosion rate in the perforated tubing

Author Biographies

Harris Prabowo, Universitas Indonesia Kampus Baru UI-Depok, Indonesia

Master of Science, Doctorate Candidate

Department of Metallurgy and Materials

Yudha Pratesa, Universitas Indonesia Kampus Baru UI-Depok, Indonesia

Master of Engineering

Department of Metallurgy and Materials

Askin Tohari, PT Pertamina Geothermal Energy Jl. Medan Merdeka Timur, 1A, Jakarta, Indonesia, 1011

Master of Science

Ali Mudakir, PT Elnusa Jl. TB Simatupang Kav. 1 B, Graha Elnusa, Jakarta, Indonesia, 12560

Master of Science

Badrul Munir, Universitas Indonesia Kampus Baru UI-Depok, Indonesia

Associate Professor

Department of Metallurgy and Materials

Johny W. Soedarsono, Universitas Indonesia Kampus Baru UI-Depok, Indonesia

Professor

Department of Metallurgy and Materials

References

  1. Teodoriu, C. (2015). Why and When Does Casing Fail in Geothermal Wells: a Surprising Question? Proceedings World Geothermal Congress 2015. Melbourne. Available at: https://pangea.stanford.edu/ERE/db/WGC/papers/WGC/2015/21041.pdf
  2. Nogara, J., Zarrouk, S. J. (2018). Corrosion in geothermal environment Part 2: Metals and alloys. Renewable and Sustainable Energy Reviews, 82, 1347–1363. doi: https://doi.org/10.1016/j.rser.2017.06.091
  3. Seiersten, M., Nyborg, R. (2016). Modelling CO2 Corrosion in Geothermal Systems. Proceedings of the Eurocorr. Available at: http://eurocorr.efcweb.org/2016/abstracts/WS%20C/67987.pdf
  4. Lyons, W. C., Stanley, J. H., Sinisterra, F. J., Weller, T. (2020). Air and Gas Drilling Manual: Applications for Oil, Gas, Geothermal Fluid Recovery Wells, Specialized Construction Boreholes, and the History and Advent of the Directional DTH. Gulf Professional Publishing, 560. doi: https://doi.org/10.1016/c2017-0-02316-9
  5. Zhong, X., Wang, Y., Liang, J., Chen, L., Song, X. (2018). The Coupling Effect of O2 and H2S on the Corrosion of G20 Steel in a Simulating Environment of Flue Gas Injection in the Xinjiang Oil Field. Materials, 11 (9), 1635. doi: https://doi.org/10.3390/ma11091635
  6. Hua, Y., Barker, R., Neville, A. (2015). Understanding the Influence of SO2 and O2 on the Corrosion of Carbon Steel in Water-Saturated Supercritical CO2. CORROSION, 71 (5), 667–683. doi: https://doi.org/10.5006/1504
  7. Hua, Y., Barker, R., Bermperidis, G., Zhao, H., Zhang, L., Neville, A. (2016). Comparison of corrosion behavior of X65, 1Cr, 5Cr and 13Cr steels in water-containing supercritical CO2 environments with SO2/O2. Proceedings of Corrosion 2016. Vancouver. Available at: https://eprints.whiterose.ac.uk/101194/3/NACE_2016_FIONAL.pdf
  8. Kermani, M. B., Morshed, A. (2003). Carbon Dioxide Corrosion in Oil and Gas Production – A Compendium. CORROSION, 59 (8), 659–683. doi: https://doi.org/10.5006/1.3277596
  9. Kermani, B., Martin, J. W., Esaklul, K. A. (2006). Materials design strategy: effects of H2S/CO2 corrosion on materials selection. CORROSION 2006. NACE International.
  10. Iannuzzi, M. (2011). Environmentally assisted cracking (EAC) in oil and gas production. Stress Corrosion Cracking, 570–607. doi: https://doi.org/10.1533/9780857093769.4.570
  11. Sardisco, J. B., Pitts, R. E. (1965). Corrosion of Iron in an H2S-CO2-H2O System Mechanism of Sulfide Film Formation and Kinetics of Corrosion Reaction. CORROSION, 21 (8), 245–253. doi: https://doi.org/10.5006/0010-9312-21.8.245
  12. Shi, F., Zhang, L., Yang, J., Lu, M., Ding, J., Li, H. (2016). Polymorphous FeS corrosion products of pipeline steel under highly sour conditions. Corrosion Science, 102, 103–113. doi: https://doi.org/10.1016/j.corsci.2015.09.024
  13. Deffo Ayagou, M. D., Joshi, G. R., Mai Tran, T. T., Tribollet, B., Sutter, E., Mendibide, C. et. al. (2020). Impact of oxygen contamination on the electrochemical impedance spectroscopy of iron corrosion in H2S solutions. Corrosion Science, 164, 108302. doi: https://doi.org/10.1016/j.corsci.2019.108302
  14. Song, Y., Palencsár, A., Svenningsen, G., Kvarekvål, J., Hemmingsen, T. (2012). Effect of O2 and Temperature on Sour Corrosion. CORROSION, 68 (7), 662–671. doi: https://doi.org/10.5006/0341
  15. Fang, H., Young, D., Nesic, S. (2008). Corrosion of mild steel in the presence of elemental sulfur. NACE - International Corrosion Conference Series. Available at: http://www.icmt.ohio.edu/documents/publications/8172.pdf
  16. Xiang, Y., Wang, Z., Xu, C., Zhou, C., Li, Z., Ni, W. (2011). Impact of SO2 concentration on the corrosion rate of X70 steel and iron in water-saturated supercritical CO2 mixed with SO2. The Journal of Supercritical Fluids, 58 (2), 286–294. doi: https://doi.org/10.1016/j.supflu.2011.06.007
  17. Xiang, Y., Wang, Z., Li, Z., Ni, W. D. (2013). Effect of temperature on corrosion behaviour of X70 steel in high pressure CO2/SO2/O2/H2O environments. Corrosion Engineering, Science and Technology, 48 (2), 121–129. doi: https://doi.org/10.1179/1743278212y.0000000050
  18. Hua, Y., Barker, R., Neville, A. (2015). The influence of SO2 on the tolerable water content to avoid pipeline corrosion during the transportation of supercritical CO2. International Journal of Greenhouse Gas Control, 37, 412–423. doi: https://doi.org/10.1016/j.ijggc.2015.03.031
  19. Sun, C., Sun, J., Wang, Y., Lin, X., Li, X., Cheng, X., Liu, H. (2016). Synergistic effect of O2, H2S and SO2 impurities on the corrosion behavior of X65 steel in water-saturated supercritical CO2 system. Corrosion Science, 107, 193–203. doi: https://doi.org/10.1016/j.corsci.2016.02.032

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Published

2020-12-31

How to Cite

Prabowo, H., Pratesa, Y., Tohari, A., Mudakir, A., Munir, B., & Soedarsono, J. W. (2020). Failure analysis of geothermal perforated casing tubing in H2S and O2 containing environment. Eastern-European Journal of Enterprise Technologies, 6(12 (108), 72–78. https://doi.org/10.15587/1729-4061.2020.215163

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Section

Materials Science