Synthesis and characterisation of dye­intercalated nickel­aluminium layered­double hydroxide as a cosmetic pigment

Authors

  • Vadym Kovalenko Ukrainian State University of Chemical Technology Gagarina ave., 8, Dnipro, Ukraine, 49005 Vyatka State University Moskovskaya str., 36, Kirov, Russian Federation, 610000, Ukraine https://orcid.org/0000-0002-8012-6732
  • Valerii Kotok Ukrainian State University of Chemical Technology Gagarina ave., 8, Dnipro, Ukraine, 49005 Vyatka State University Moskovskaya str., 36, Kirov, Russian Federation, 610000, Ukraine https://orcid.org/0000-0001-8879-7189
  • Anastasiya Yeroshkina Ukrainian State University of Chemical Technology Gagarina ave., 8, Dnipro, Ukraine, 49005, Ukraine https://orcid.org/0000-0002-6293-3557
  • Alexander Zaychuk Ukrainian State University of Chemical Technology Gagarina ave., 8, Dnipro, Ukraine, 49005, Ukraine https://orcid.org/0000-0001-5209-7498

DOI:

https://doi.org/10.15587/1729-4061.2017.109814

Keywords:

cosmetic pigment, murexide, Ni­Al LDH, chemisorption, intercalation, nail polish

Abstract

Dye­intercalated layered double hydroxides (LDH) are modern promising pigments for paint and cosmetics industry. For the preparation of high­quality cosmetic pigments, particularly for nail polish, it was proposed to use not only intercalation but also chemisorption. For the pigment synthesis, Ni­AL LDH was chosen, along with murexide (Ammonium (purpurate) 2,6­dioxo­5­[(2,4,6­trioxo­5­hexahydropyrimidinylidene)amino]­3H­pyrimidin­4­olate), in which colored purpurate anion is able to form complex compounds with Ni2+. The murexide­intercalated (murexide amount for intercalation only) and murexide­intercalated­chemisorbed (murexide amount for Ni2+) Ni­Al LDH pigments were synthesized and used for the preparation of nail polish samples. The crystallographic composition was studied by means of XRD analysis. The color parameters (coordinates of color and chromaticity, dominant wavelength and color purity) of pigment powders and nail polish samples with these pigments have been studied using a color comparator. Organoleptic characteristics of pigment and nail polish samples were studied. The positive influence of chemisorption was shown: murexide­intercalated­chemisorbed pigment is easily ground, with the formation of highly dispersed powder, which during the preparation of nail polish was easily dispersed with the formation of stable yellow samples (dominant wavelength 583 nm) with high color purity of 43 %. Also, high covering ability of the murexide­intercalated­chemisorbed pigment was shown: high­quality, opaque, colored nail polish coat was formed at the pigment content of 45 %, 30 % and 15 % (wt.). For the synthesis of such pigments, it was recommended to choose anionic dyes that can form coordination bonds with LDH cations.

Author Biographies

Vadym Kovalenko, Ukrainian State University of Chemical Technology Gagarina ave., 8, Dnipro, Ukraine, 49005 Vyatka State University Moskovskaya str., 36, Kirov, Russian Federation, 610000

PhD, Associate Professor

Department of Analytical Chemistry and Food Additives and Cosmetics

Department of Technologies of Inorganic Substances and Electrochemical Manufacturing

Valerii Kotok, Ukrainian State University of Chemical Technology Gagarina ave., 8, Dnipro, Ukraine, 49005 Vyatka State University Moskovskaya str., 36, Kirov, Russian Federation, 610000

PhD, Associate Professor

Department of Processes, Apparatus and General Chemical Technology

Department of Technologies of Inorganic Substances and Electrochemical Manufacturing

Anastasiya Yeroshkina, Ukrainian State University of Chemical Technology Gagarina ave., 8, Dnipro, Ukraine, 49005

Department of Analytical Chemistry and Food Additives and Cosmetics

Alexander Zaychuk, Ukrainian State University of Chemical Technology Gagarina ave., 8, Dnipro, Ukraine, 49005

Doctor of Technical Sciences, Associate Professor

Department of Chemical Technology of Ceramics and Glass 

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Published

2017-10-31

How to Cite

Kovalenko, V., Kotok, V., Yeroshkina, A., & Zaychuk, A. (2017). Synthesis and characterisation of dye­intercalated nickel­aluminium layered­double hydroxide as a cosmetic pigment. Eastern-European Journal of Enterprise Technologies, 5(12 (89), 27–33. https://doi.org/10.15587/1729-4061.2017.109814

Issue

Vol. 5 No. 12 (89) (2017): MATERIALS SCIENCE

Section

Materials Science

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Copyright (c) 2017 Vadym Kovalenko, Valerii Kotok, Anastasiya Yeroshkina, Alexander Zaychuk

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