Determining the influence of technological factors on the microstructural and rheological parameters of sauces with emulsion structure
DOI:
https://doi.org/10.15587/1729-4061.2025.325417Keywords:
sauces with an emulsion structure, heat treatment, microstructural indicators, rheological indicatorsAbstract
The object of this study is hot sauces with an emulsion structure, namely their microstructural and rheological indicators. The principal task addressed in the study is to identify the possibility of two-cycle heat treatment of sauces with maximum preservation of their properties. This could significantly expand their technological use, in particular, as part of ready-to-eat meals of industrial production. This approach contributes to the justification of the technological use of sauces while simultaneously determining the indicators that are control points in the technological flow of their production.
Studies on the microstructure of sauces have demonstrated a bimodal nature of the particle distribution with two pronounced peaks, which are in the range of 2.42–4.03 μm and 31.10–36.30 μm. The SPAN index is in the range of 1.62–1.72, reflecting moderate polydispersity. One- and two-cycle heat treatment of sauces contributes to a decrease in the specific surface area and an increase in the values of the volume-surface diameter of particles, which indicates a change in the microstructural characteristics of sauces. Sauces are structured food systems that demonstrate typical non-Newtonian behavior. During cyclic heat treatment of sauces, there is an increase in viscosity, storage moduli, and losses in the series "freshly made sauce®sauce after 1 heat treatment cycle®sauce after 2 heat treatment cycles".
A distinctive feature of the experimental results relates to studying sauces that are consumed hot, which determines additional requirements for their stability. The technological solutions proposed in this paper are aimed at their production in the form of semi-finished products with a high degree of readiness
References
- Klymenko, N., Voronenko, I., Nehrey, M., Rogoza, K., Rogoza, N. (2023). Risk assessment of shock periods and investment attractiveness of agroholdings of Ukraine. Agricultural and Resource Economics: International Scientific E-Journal, 9 (2). https://doi.org/10.51599/are.2023.09.02.07
- Ivanov, V., Shevchenko, O., Marynin, A., Stabnikov, V., Gubenia, O., Stabnikova, O. et al. (2021). Trends and expected benefits of the breaking edge food technologies in 2021–2030. Ukrainian Food Journal, 10 (1), 7–36. https://doi.org/10.24263/2304-974x-2021-10-1-3
- Market Research Report on Sauces n Ukraine. 2025 Year. Available at: https://pro-consulting.ua/en/issledovanie-rynka/analiz-rynka-sousov-v-ukraine-2025-god
- Goralchuk, A., Grinchenko, O., Riabets, O., Kotlyar, О. (2019). Food dispersion systems process stabilization. A review. Ukrainian Food Journal, 8 (4), 699–732. https://doi.org/10.24263/2304-974x-2019-8-4-4
- Krstonošić, V., Dokić, L., Nikolić, I., Milanović, M. (2015). Influence of xanthan gum on oil-in-water emulsion characteristics stabilized by OSA starch. Food Hydrocolloids, 45, 9–17. https://doi.org/10.1016/j.foodhyd.2014.10.024
- Agama-Acevedo, E., Bello-Perez, L. A. (2017). Starch as an emulsions stability: the case of octenyl succinic anhydride (OSA) starch. Current Opinion in Food Science, 13, 78–83. https://doi.org/10.1016/j.cofs.2017.02.014
- Hedayati, S., Shahidi, F., Koocheki, A., Farahnaky, A., Majzoobi, M. (2020). Influence of pregelatinized and granular cold water swelling maize starches on stability and physicochemical properties of low fat oil-in-water emulsions. Food Hydrocolloids, 102, 105620. https://doi.org/10.1016/j.foodhyd.2019.105620
- Hrynchenko, O., Radchenko, A., Dehtiar, V., Grynchenko, N., Serik, M. (2025). Development of technology for food products with emulsion structure based on pea groats and pea aquafaba. Eastern-European Journal of Enterprise Technologies, 1 (11 (133)), 17–27. https://doi.org/10.15587/1729-4061.2025.323339
- Jo, M., Chang, M. J., Goh, K. K. T., Ban, C., Choi, Y. J. (2021). Rheology, Microstructure, and Storage Stability of Emulsion-Filled Gels Stabilized Solely by Maize Starch Modified with Octenyl Succinylation and Pregelatinization. Foods, 10 (4), 837. https://doi.org/10.3390/foods10040837
- Degner, B. M. (2013) Freeze stabilty enhancement of dairy emulsions by microparticulated whey protein. ETD collection for University of Nebraska-Lincoln. AAI3603563. Available at: https://digitalcommons.unl.edu/dissertations/AAI3603563
- Ianushkevich, O., Grynchenko, N. (2023). Justification of the choice of food ingredients for obtaining thermostable emulsion systems as the basis of hot sauces. Science Bulletin of Poltava University of Economics and Trade. Series "Technical Sciences", 1, 19–24. Available at: http://puet.poltava.ua/index.php/technical/article/view/189
- Hernández-Carrión, M., Guardeño, L. M., Carot, J. M., Pérez-Munuera, I., Quiles, A., Hernando, I. (2011). Structural stability of white sauces prepared with different types of fats and thawed in a microwave oven. Journal of Food Engineering, 104 (4), 557–564. https://doi.org/10.1016/j.jfoodeng.2011.01.017
- Ramirez-Sucre, M. O., Allende, D. B. (2016). Effect of Thermal Treatment on the Rheological Behavior of Habanero Chili (Capsicum chinense) Sauces Added with Guar and Xanthan Gums. Agrociencia, 50 (7), 837–847. Available at: https://www.scielo.org.mx/scielo.php?script=sci_arttext&pid=S1405-31952016000700837&lng=es&nrm=iso&tlng=en
- Herranz, B., Martínez, A., Alvarez, M. D. (2019). Influence of Fiber Addition on White Sauces Made with Corn Starch: Effect on Their Freezing/Thawing Stability. Journal of Food Science, 84 (8), 2128–2138. https://doi.org/10.1111/1750-3841.14700
- McClements, D. J. (2015). Food Emulsions. CRC Press. https://doi.org/10.1201/b18868
- Alvarez, M., Fuentes, R., Canet, W. (2015). Effects of Pressure, Temperature, Treatment Time, and Storage on Rheological, Textural, and Structural Properties of Heat-Induced Chickpea Gels. Foods, 4 (2), 80–114. https://doi.org/10.3390/foods4020080
- Sudheesh, C., Sunooj, K. V., Sinha, S. K., George, J., Kumar, S., Murugesan, P. et al. (2019). Impact of energetic neutral nitrogen atoms created by glow discharge air plasma on the physico-chemical and rheological properties of kithul starch. Food Chemistry, 294, 194–202. https://doi.org/10.1016/j.foodchem.2019.05.067
- Guimarães, C. F., Gasperini, L., Ribeiro, R. S., Carvalho, A. F., Marques, A. P., Reis, R. L. (2020). High-throughput fabrication of cell-laden 3D biomaterial gradients. Materials Horizons, 7 (9), 2414–2421. https://doi.org/10.1039/d0mh00818d
- Mezger, T. G. (2012). The Rheology Handbook. Vincentz Network. https://doi.org/10.1515/9783748600367
- Bortnowska, G., Balejko, J., Tokarczyk, G., Romanowska-Osuch, A., Krzemińska, N. (2014). Effects of pregelatinized waxy maize starch on the physicochemical properties and stability of model low-fat oil-in-water food emulsions. Food Hydrocolloids, 36, 229–237. https://doi.org/10.1016/j.foodhyd.2013.09.012
- Yanushkevych, O. I., Hrynchenko, N. H. (2023). Study of the influence of technological factors on the viscosity of pasteurized dispersions of native and modified starches. Food production equipment and technologies, 1 (46), 26–33. Available at: https://oblad.donnuet.edu.ua/index.php/tehnolog/article/view/204/179
Downloads
Published
How to Cite
Issue
Section
License
Copyright (c) 2025 Oleksandr Ianushkevych, Nataliya Grynchenko, Anna Radchenko, Iryna Smetanska, Andrii Marynin, Olha Hrynchenko

This work is licensed under a Creative Commons Attribution 4.0 International License.
The consolidation and conditions for the transfer of copyright (identification of authorship) is carried out in the License Agreement. In particular, the authors reserve the right to the authorship of their manuscript and transfer the first publication of this work to the journal under the terms of the Creative Commons CC BY license. At the same time, they have the right to conclude on their own additional agreements concerning the non-exclusive distribution of the work in the form in which it was published by this journal, but provided that the link to the first publication of the article in this journal is preserved.
A license agreement is a document in which the author warrants that he/she owns all copyright for the work (manuscript, article, etc.).
The authors, signing the License Agreement with TECHNOLOGY CENTER PC, have all rights to the further use of their work, provided that they link to our edition in which the work was published.
According to the terms of the License Agreement, the Publisher TECHNOLOGY CENTER PC does not take away your copyrights and receives permission from the authors to use and dissemination of the publication through the world's scientific resources (own electronic resources, scientometric databases, repositories, libraries, etc.).
In the absence of a signed License Agreement or in the absence of this agreement of identifiers allowing to identify the identity of the author, the editors have no right to work with the manuscript.
It is important to remember that there is another type of agreement between authors and publishers – when copyright is transferred from the authors to the publisher. In this case, the authors lose ownership of their work and may not use it in any way.





