The identification of hydrogen embrittlement and the role of intergranular brittle fracture of API 5DP G105 drill pipe failure on onshore drilling activity

Authors

DOI:

https://doi.org/10.15587/1729-4061.2026.361514

Keywords:

high-density completion fluid, hydrogen embrittlement, high-strength steel failure analysis, drilling completion

Abstract

The object of this study is high-strength steel of API 5DP Gr 105 that has been used during well completion in a corrosive environment. This work emphasizes key factors affecting material damage caused by slip marks, tensile load, and hydrogen content in contaminated brine and completion fluid, which were not addressed in previous studies. Several tests, including chemical, mechanical, and surface characterization, were conducted. The chemical composition test of the fluid shows that the brine has been contaminated by H2S gas and sulfur, with inevitable traces of chloride, bicarbonate, carbonate, bisulfide, and sulfide, providing active sites for hydrogen atom diffusion at the slip marks. The material composition test confirms that the failed material is API 5DP Gr 105. A noticeable amount of phosphorus increases grain boundary segregation and weakens the cohesive metallic bond. A hardness at 28 Rockwell C is inevitable and increases the material’s vulnerability to embrittlement, despite the Charpy energy test showing a manageable level, confirming local brittleness. The high tensile strength of 914 MPa is evidence of embrittlement, even though the material remains ductile, with a noticeable elongation of 20%. An intergranular crack was observed in the microstructure, and slip marks serve as stress concentrators for the crack. Thus, it can be concluded that the combination of tensile load, hydrogen gas content, local slip marks, and completion fluid in the well weakened the grain boundaries and served as an initial crack with a high hydrogen-atom concentration. This work models the root-cause analysis of high-strength steel during well-completion operations in an onshore facility

Author Biographies

Sidhi Aribowo, University of Indonesia

PhD Student

Department of Materials and Metallurgical Engineering

Johny Wahyuadi Soedarsono, Universitas Indonesia

Doctor of Engineering, Professor

Prof Johny Wahyuadi Laboratory

Department of Metallurgical and Materials Engineering

Suryadi Suryadi, Universitas Indonesia

Head of Engineering Services Division

Center for Materials Processing and Failure Analysis (CMPFA)

Department of Metallurgical and Materials Engineering

Slamet Nurhadi, Pertamina Drilling Services Indonesia

Maintenance Manager

Warneri Warneri, Pertamina Drilling Services Indonesia

Manager Rig Operation V

Sopar Mangarapot Simanullang, Pertamina Drilling Services Indonesia

Assistant Manager Quality Control

Agus Kaban, Universitas Indonesia

Master of Engineering, Graduate Student

Prof Johny Wahyuadi Laboratory

Department of Metallurgical and Materials Engineering

Raajwa Ayudhia Kamila, Universitas Indonesia

Research Assistant

Prof Johny Wahyuadi Laboratory

Department of Metallurgical and Materials Engineering

References

  1. Laureys, A., Depraetere, R., Cauwels, M., Depover, T., Hertelé, S., Verbeken, K. (2022). Use of existing steel pipeline infrastructure for gaseous hydrogen storage and transport: A review of factors affecting hydrogen induced degradation. Journal of Natural Gas Science and Engineering, 101, 104534. https://doi.org/10.1016/j.jngse.2022.104534
  2. Aditiyawarman, T., Soedarsono, J. W., Kaban, A. P. S., Riastuti, R., Rahmadani, H. (2022). The Study of Artificial Intelligent in Risk-Based Inspection Assessment and Screening: A Study Case of Inline Inspection. ASCE-ASME Journal of Risk and Uncertainty in Engineering Systems, Part B: Mechanical Engineering, 9 (1). https://doi.org/10.1115/1.4054969
  3. Sridharan, V. S., Verma, V. K., Narayan, R. L., Lu, X., Siwei, D., Chaudhary, V. et al. (2025). Hydrogen embrittlement of additively manufactured metallic materials. International Journal of Hydrogen Energy, 121, 245–272. https://doi.org/10.1016/j.ijhydene.2025.03.222
  4. Mokhtari, E., Heidarpour, A., Javidan, F. (2024). Mechanical performance of high strength steel under corrosion: A review study. Journal of Constructional Steel Research, 220, 108840. https://doi.org/10.1016/j.jcsr.2024.108840
  5. Oriani, R. A. (1972). A mechanistic theory of hydrogen embrittlement of steels. Berichte Der Bunsengesellschaft Für Physikalische Chemie, 76 (8), 848–857. Portico. https://doi.org/10.1002/bbpc.19720760864
  6. Damage Mechanisms Affecting fixed Equipment in the Refining Industry (2003). Recommended Practice 571 First Edition. API.
  7. Wu, X., Song, Z., Tan, M., Jia, W., Liu, J. (2026). Hydrogen-induced failure mechanism of X80 pipeline steel welded joints based on macro-and micro-scale experimental analysis: Embrittlement enhancement effect caused by high hydrogen trap density. Engineering Failure Analysis, 183, 110190. https://doi.org/10.1016/j.engfailanal.2025.110190
  8. Zekun, Y., Zhanli, Y., Hao, Y., Yan, Z., Kai, X. (2025). Hydrogen embrittlement in welded joints of high-strength pipeline steels: A review of mechanisms, characterization, and mitigation strategies. International Journal of Pressure Vessels and Piping, 218, 105615. https://doi.org/10.1016/j.ijpvp.2025.105615
  9. Kawamori, M., Shibata, K., Yoda, R., Morita, S., Fujita, Y., Kuroda, S. et al. (2025). Dual effects of deformation on hydrogen embrittlement of austenitic stainless steels revealed by hydrogen visualization combined with microstructural analysis. International Journal of Hydrogen Energy, 145, 559–577. https://doi.org/10.1016/j.ijhydene.2025.05.426
  10. Kawamori, M., Yuse, F. (2023). In-situ measurement of hydrogen entry and hydrogen embrittlement of steel by atmospheric corrosion. Corrosion Science, 219, 111212. https://doi.org/10.1016/j.corsci.2023.111212
  11. Lan, X., Okada, K., Ueji, R., Shibata, A. (2025). Improving hydrogen embrittlement resistance in high-strength martensitic steels via thermomechanical processing. Scripta Materialia, 264, 116711. https://doi.org/10.1016/j.scriptamat.2025.116711
  12. Hwang, Y., Park, H., Yun, H. S., Bae, K.-O., Baek, U. B., Lee, J. (2025). Effects of sensitization on hydrogen embrittlement behavior in 304 stainless steel. Materials & Design, 260, 115130. https://doi.org/10.1016/j.matdes.2025.115130
  13. Dong, X., Wang, D., Thoudden-Sukumar, P., Tehranchi, A., Ponge, D., Sun, B., Raabe, D. (2022). Hydrogen-associated decohesion and localized plasticity in a high-Mn and high-Al two-phase lightweight steel. Acta Materialia, 239, 118296. https://doi.org/10.1016/j.actamat.2022.118296
  14. Asadipoor, M., Pourkamali Anaraki, A., Kadkhodapour, J., Sharifi, S. M. H., Barnoush, A. (2020). Macro- and microscale investigations of hydrogen embrittlement in X70 pipeline steel by in-situ and ex-situ hydrogen charging tensile tests and in-situ electrochemical micro-cantilever bending test. Materials Science and Engineering: A, 772, 138762. https://doi.org/10.1016/j.msea.2019.138762
  15. Singh, R., Sharma, R., Rao, G. R. (2023). A comprehensive review on the high-density clear completion fluids for applications in HPHT well completion. International Journal of Oil, Gas and Coal Technology, 32 (1), 70. https://doi.org/10.1504/ijogct.2023.127337
  16. Peng, X., Yu, H., Lian, Z., Dong, B., Zhong, W., Zhang, Y., Hu, Z. (2021). Material optimization of drill pipe in complex wellbore environments by comparing fatigue life and cost. Energy Reports, 7, 5420–5430. https://doi.org/10.1016/j.egyr.2021.08.135
  17. Zamani, S. M., Hassanzadeh-Tabrizi, S. A., Sharifi, H. (2016). Failure analysis of drill pipe: A review. Engineering Failure Analysis, 59, 605–623. https://doi.org/10.1016/j.engfailanal.2015.10.012
  18. Atamashkin, A., Priymak, E., Tulibaev, E., Syomka, Y., Trushov, V. (2024). Influence of force parameters of rotary friction welding on the microstructure and mechanical properties of welded joints of high-strength drill pipes. International Journal on Interactive Design and Manufacturing, 19 (4), 2937–2950. https://doi.org/10.1007/s12008-024-02011-w
  19. Cho, L., Bradley, P. E., Lauria, D. S., Connolly, M. J., Seo, E. J., Findley, K. O. et al. (2021). Effects of hydrogen pressure and prior austenite grain size on the hydrogen embrittlement characteristics of a press-hardened martensitic steel. International Journal of Hydrogen Energy, 46 (47), 24425–24439. https://doi.org/10.1016/j.ijhydene.2021.05.005
  20. Yu, H., He, J., Morin, D. D., Ortiz, M., Zhang, Z. (2025). A self-consistent void-based rationale for hydrogen embrittlement. Scripta Materialia, 255, 116403. https://doi.org/10.1016/j.scriptamat.2024.116403
  21. Kim, K.-S., Kang, J.-H., Kim, S.-J. (2019). Effect of Grain Boundary Carbide on Hydrogen Embrittlement in Stable Austenitic Stainless Steels. ISIJ International, 59 (6), 1136–1144. https://doi.org/10.2355/isijinternational.isijint-2018-639
  22. Puiggali, M., Zielinski, A., Olive, J. M., Renauld, E., Desjardins, D., Cid, M. (1998). Effect of microstructure on stress corrosion cracking of an Al-Zn-Mg-Cu alloy. Corrosion Science, 40 (4-5), 805–819. https://doi.org/10.1016/s0010-938x(98)00002-x
  23. Howard, S., Chrenowski, M. (2014). Corrosion in Formate Brines – 20 Years of Laboratory Testing and Field Experience. Offshore Technology Conference-Asia. https://doi.org/10.4043/24983-ms
  24. Silverman, S. A., Bhavsar, R., Edwards, C., Virally, S., Foxenberg, W. (2003). Use of High-Strength Alloys and Elastomers in Heavy Completion Brines. SPE Annual Technical Conference and Exhibition. https://doi.org/10.2118/84515-ms
  25. Espinosa-Medina, M. A., la Torre, G. C.-D., Castillo, A. S., Ángeles-Chávez, C., Zeferino-Rodríguez, T., González-Rodríguez, J. G. (2017). Effect of Chloride and Sulfate Ions on the SCC of API-X70 Pipeline Welds in Diluted Carbonated Solutions. International Journal of Electrochemical Science, 12 (8), 6952–6965. https://doi.org/10.20964/2017.08.07
  26. Komazazki, S.-I., Watanabe, S., Misawa, T. (2003). Influence of Phosphorus and Boron on Hydrogen Embrittlement Susceptibility of High Strength Low Alloy Steel. ISIJ International, 43 (11), 1851–1857. https://doi.org/10.2355/isijinternational.43.1851
  27. Nanninga, N., Grochowsi, J., Heldt, L., Rundman, K. (2010). Role of microstructure, composition and hardness in resisting hydrogen embrittlement of fastener grade steels. Corrosion Science, 52 (4), 1237–1246. https://doi.org/10.1016/j.corsci.2009.12.020
  28. Park, H., Yoo, J., Lee, J.-J., Kang, Y., Seo, K. M., Lee, C.-H. et al. (2024). Impact of hydrogen embrittlement on the tensile-shear property of resistance spot-welded advanced high-strength martensitic steels. International Journal of Hydrogen Energy, 71, 319–333. https://doi.org/10.1016/j.ijhydene.2024.05.138
  29. Li, X., Zhang, J., Cui, Y., Djukic, M. B., Feng, H., Wang, Y. (2024). Review of the hydrogen embrittlement and interactions between hydrogen and microstructural interfaces in metallic alloys: Grain boundary, twin boundary, and nano-precipitate. International Journal of Hydrogen Energy, 72, 74–109. https://doi.org/10.1016/j.ijhydene.2024.05.257
  30. Cui, D., Bai, Y., Xiong, L., Yu, B., Wei, B., Sun, C. (2024). Effects of hydrogen blending ratios and CO2 on hydrogen embrittlement of X65 steel in high-pressure offshore hydrogen-blended natural gas pipelines. Journal of Materials Research and Technology, 33, 4763–4771. https://doi.org/10.1016/j.jmrt.2024.10.150
  31. Tong, Z., Wang, H., Zheng, W., Zhou, H. (2024). Change in Hydrogen Trapping Characteristics and Influence on Hydrogen Embrittlement Sensitivity in a Medium-Carbon, High-Strength Steel: The Effects of Heat Treatments. Materials, 17 (8), 1854. https://doi.org/10.3390/ma17081854
The identification of hydrogen embrittlement and the role of intergranular brittle fracture of API 5DP G105 drill pipe failure on onshore drilling activity

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Published

2026-06-30

How to Cite

Aribowo, S., Soedarsono, J. W., Suryadi, S., Nurhadi, S., Warneri, W., Simanullang, S. M., Kaban, A., & Kamila, R. A. (2026). The identification of hydrogen embrittlement and the role of intergranular brittle fracture of API 5DP G105 drill pipe failure on onshore drilling activity. Eastern-European Journal of Enterprise Technologies, 3(1 (141), 53–63. https://doi.org/10.15587/1729-4061.2026.361514

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Section

Engineering technological systems